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By Nagnibida N. I.

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As we shall later see, there are also lock and decoupler channels that operate in a similar manner. Next, we will expand on these and other aspects of the N M R experiment in greater detail. 1). The magnetic field can be supplied by one of three types of magnets: permanent magnets, electromagnets, or superconducting magnets. The magnetic field for an N M R experiment must be stable and homogeneous, conditions that are met by locking and shimming the field. 1 Permanent Magnets N M R spectrometers that are designed around permanent magnets are generally rugged and inexpensive.

The magnetic field for an N M R experiment must be stable and homogeneous, conditions that are met by locking and shimming the field. 1 Permanent Magnets N M R spectrometers that are designed around permanent magnets are generally rugged and inexpensive. 4 Τ [1 Τ (tesla) — 10 kG (kilogauss)] is about the maximum strength for such systems. A permanent magnet must be encased in some type of insulated housing to prevent temperature-induced drifts in the magnetic field. Because of field drift problems such systems are not ideal for long spectral accumulations.

Thus, in N M R spectroscopy, in contrast to optical spectroscopy, there is no natural fundamental scale unit; the energies of transitions between quantum levels are proportional to the laboratory field. There is also no natural zero of reference. For practical purposes, these difficulties are evaded by these devices: a. Using parts per million relative change in B Q or i> as the scale unit. ) b. Using an arbitrary reference substance dissolved in the sample and referring all displacements in resonance, called chemical shifts, to this "internal" reference.

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A basis for the space of functions analytic in a disk by Nagnibida N. I.


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